Presenter(s)

Catherine Braaten, Kezia Lemke, Elijah Murray, and Leighton Stouffer

Abstract

Rhodamine B dye is a harmful contaminant in wastewater, so methods were developed to synthesize iron oxide nanoparticles that could catalyze the photodegradation of rhodamine B in water. Iron oxide nanoparticles were synthesized through the co-precipitation method and using FeCl2 as a source of Fe2+ ions. The nanoparticles were then characterized through IR spectroscopy and adsorption testing. Finally, a control solution of rhodamine B and an experimental rhodamine B solution with nanoparticles were exposed to UV light in a photo cabinet to analyze the degradation of rhodamine B over time using UV-Vis spectroscopy. IR spectroscopy showed that an iron oxide material had been synthesized, and adsorption testing revealed that rhodamine B adsorption equilibrium occurred around 95 min. The equilibrium dye adsorption Q value was 0.44 mg/g on the nanoparticles. The photocatalysis experiment showed little difference between the control and experimental solutions, with slopes of -1.5×10-3 mg/(L×min) and -1.7×10-3 mg/(L×min), respectively, and poor linearity with R2 values of 0.32 and 0.28, respectively. Overall, the results illustrate that an iron oxide nanoparticle material was synthesized and it was able to adsorb a moderate amount of rhodamine B. However, there was little degradation of rhodamine B in both the experimental and control solutions with almost no enhanced catalysis due to the presence of iron oxide nanoparticles.

College

College of Science & Engineering

Department

Chemistry

Campus

Winona

First Advisor/Mentor

Jennifer Zemke

Location

Kryzsko Great River Ballroom, Winona, Minnesota; United States

Start Date

4-23-2026 1:00 PM

End Date

4-23-2026 2:00 PM

Presentation Type

Poster Session

Format of Presentation or Performance

In-Person

Session

2a=1pm-2pm

Poster Number

63

Comments

Lemke, Kezia J; Murray, Elijah J; Stouffer, Leighton D; Braaten, Catherine S

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Apr 23rd, 1:00 PM Apr 23rd, 2:00 PM

Synthesis of Iron Oxide Nanoparticles for the Degradation of Rhodamine B Dye

Kryzsko Great River Ballroom, Winona, Minnesota; United States

Rhodamine B dye is a harmful contaminant in wastewater, so methods were developed to synthesize iron oxide nanoparticles that could catalyze the photodegradation of rhodamine B in water. Iron oxide nanoparticles were synthesized through the co-precipitation method and using FeCl2 as a source of Fe2+ ions. The nanoparticles were then characterized through IR spectroscopy and adsorption testing. Finally, a control solution of rhodamine B and an experimental rhodamine B solution with nanoparticles were exposed to UV light in a photo cabinet to analyze the degradation of rhodamine B over time using UV-Vis spectroscopy. IR spectroscopy showed that an iron oxide material had been synthesized, and adsorption testing revealed that rhodamine B adsorption equilibrium occurred around 95 min. The equilibrium dye adsorption Q value was 0.44 mg/g on the nanoparticles. The photocatalysis experiment showed little difference between the control and experimental solutions, with slopes of -1.5×10-3 mg/(L×min) and -1.7×10-3 mg/(L×min), respectively, and poor linearity with R2 values of 0.32 and 0.28, respectively. Overall, the results illustrate that an iron oxide nanoparticle material was synthesized and it was able to adsorb a moderate amount of rhodamine B. However, there was little degradation of rhodamine B in both the experimental and control solutions with almost no enhanced catalysis due to the presence of iron oxide nanoparticles.

 

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